Welcome to Yantai Dasteck Chemicals Co., Ltd. Contact  |  English / 中文
Home > FAQ > How should a substitution trial be recorded and reported?

How should a substitution trial be recorded and reported?

Direct answer

Without a proper record, a substitution trial cannot say clearly whether it worked. A usable trial report only has to answer four things: what the starting recipe was, which levels were tried, how each one performed, and whether it can be scaled up. The framework below can be used directly.

1. Conditions to fix before starting

ItemRequirement
Machine and liquor ratioRecord the machine and liquor ratio; do not mix machines in one trial
FabricSame greige lot, with article number and weight recorded
WaterRecord hardness or conductivity; use softened water if needed
Temperature and timeKeep constant across levels; change only the variable under test
AlkaliFixed by the trial plan; never cut in proportion to the reducer

2. Suggested trial levels

Use the hydrosulfite recipe as the control and set three or four substitution levels, for example:

  • Control: 100% hydrosulfite
  • Level 1: substitute one quarter
  • Level 2: substitute one half
  • Level 3: substitute three quarters or all of it

For each level record the dose in both g/L and g/kg on fabric, plus pH, temperature, time and ORP where available.

3. Results to measure at every level

CategoryFigures
EffectWhiteness, or colour yield as K/S, plus a* and b*
QualityWash and rub fastness, strength, hand (add elastic recovery where elastane is present)
ProcessActual dose, alkali consumption, heating time, total time
CostChemical cost per tonne of fabric or per oven-dry tonne of pulp

4. How to write the conclusion

1. Whether substitution is possible: which level met the target and which did not

2. Scale-up risk: what to watch if machine, liquor ratio or water changes

3. Next step: whether a pilot is needed and which conditions it must fix

4. Retention and attachments: sample photographs, COA and test data attached

5. Three commonly missed records

  • Alkali: watching only the reducer change and ignoring the alkali distorts the conclusion
  • ORP: recording the dose but not the potential makes scale-up impossible to reproduce
  • Rinsing and neutralising: differences here often outweigh the difference between the reducers themselves

Sources

The framework follows standard laboratory and pilot-plant practice. Specific test methods must follow your own or the customer standard.